Analytical method for the determination of dimethylsulfamoyl chloride
Translation of DGUV Information 213-543 (former BGI 505-43 or ZH1/120.43)
CAS Number:13360-57-1
Method 01 – GC – limited suitability: category E1
Sampling with a pump and Adsorption on Tenax TA. Gas chromatography after desorption.
This method permits the determination of dimethylsulfamoyl chloride concentrations in working areas averaged over the sampling time after personal or stationary sampling.
Principle
With a pump a measured air volume is drawn through a glass tube filled with Tenax TA. After desorption with toluene containing hexachloroethane as internal standard,the dimethylsulfamoyl chloride is determined by gas chromatography.
Limit of quantification (LOQ)
Absolute: 0.05 ng.
Relative: 0.03 mg/m³ dimethylsulfamoyl chloride for a 15-litre air sample.
Issue
July 1989
The measuring method is of limited suitability (E1).
The complete measuring method is available in the Wiley Online Library: Method for the determination of dimethylsulfamoyl chloride (Analyses of Hazardous Substances in Air, Volume 7, 2003).
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